Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

Base Information

Chemical Name:Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside
CAS No.:81307-79-1
Molecular Formula:C₆₂H₆₆O₁₁
Molecular Weight:987.199
Hs Code.:

Synonyms:Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

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Chemical Property of Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

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Technology Process of Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside

There total 46 articles about Methyl O-(2,3,4,6-tetra-O-benzyl-α-D-galactopyranosyl)-(1->4)-2,3,6-tri-O-benzyl-β-D-galactopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 92470-93-4
(2R,3R,4S,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-chlorotetrahydro-2H-pyran

: 64694-18-4,77117-44-3,81307-79-1,82805-15-0,82805-16-1,82805-17-2,82805-18-3,84799-76-8,114817-97-9,114817-98-0,117894-99-2,123806-51-9,123877-32-7,117894-98-1
methyl 4-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside; (2R,3R,4S,5S,6R)-3,4,5-tris(benzyloxy)-2-((benzyloxy)methyl)-6-chlorotetrahydro-2H-pyran; With silver(l) oxide; In dichloromethane; at 0 ℃; for 0.166667h; Molecular sieve; Inert atmosphere;

With trifluorormethanesulfonic acid; In dichloromethane; at 0 ℃; for 0.5h; Molecular sieve; Inert atmosphere;
DOI:10.1002/chem.201905576

Reference yield: 92.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 1-O-(((1-ethynylcyclohexyl)oxy)carbonyl)-2,3,4,6-tetra-O-benzyl D-mannopyranoside

: 64694-18-4,77117-44-3,81307-79-1,82805-15-0,82805-16-1,82805-17-2,82805-18-3,84799-76-8,114817-97-9,114817-98-0,117894-99-2,123806-51-9,123877-32-7,117894-98-1
methyl 4-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With tris(2,4-di-tert-butylphenyl)phosphiteAuCl; silver trifluoromethanesulfonate; In dichloromethane; at 25 ℃; for 0.25h; Molecular sieve; Inert atmosphere;
DOI:10.1002/anie.201511695

Reference yield: 92.0%

: 19488-48-3
methyl O-2,3,6-tri-O-benzyl-α-D-glucopyranoside

: 1H-benzo[d][1,2,3]triazol-1-yl 2,3,4,6-tetra-O-benzyl α-D-mannopyranoside

: 64694-18-4,77117-44-3,81307-79-1,82805-15-0,82805-16-1,82805-17-2,82805-18-3,84799-76-8,114817-97-9,114817-98-0,117894-99-2,123806-51-9,123877-32-7,117894-98-1
methyl 4-O-(2,3,4,6-tetra-O-benzyl-α-D-mannopyranosyl)(1→4)-2,3,6-tri-O-benzyl-α-D-glucopyranoside

Guidance literature:: With trifluoromethylsulfonic anhydride; In dichloromethane; at 0 ℃; Inert atmosphere; Molecular sieve;
DOI:10.1021/acs.joc.7b02027