C₅₀H₇₂N₈O₁₂Si

Base Information

Chemical Name:C₅₀H₇₂N₈O₁₂Si
CAS No.:343332-78-5
Molecular Formula:C₅₀H₇₂N₈O₁₂Si
Molecular Weight:1005.25
Hs Code.:

C<sub>50</sub>H<sub>72</sub>N<sub>8</sub>O<sub>12</sub>Si

Synonyms:C₅₀H₇₂N₈O₁₂Si

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Chemical Property of C₅₀H₇₂N₈O₁₂Si

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Technology Process of C₅₀H₇₂N₈O₁₂Si

There total 10 articles about C₅₀H₇₂N₈O₁₂Si which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 72.0%

: 343332-76-3
C₃₁H₄₀N₆O₉

: 89106-03-6
6-benzyloxycarbonylamino-2-L-amino-hexanoic acid trimethylsilyl ethyl ester

: 343332-78-5
C₅₀H₇₂N₈O₁₂Si

Guidance literature:: With sodium tris(acetoxy)borohydride; N-ethyl-N,N-diisopropylamine; In 1,2-dichloro-ethane; at 20 ℃; for 16h;
DOI:10.1021/ja005886l

Reference yield:

: 343332-60-5
4-allylamino-6-benzyloxy-2-methylamino-pyrimidine-5-carbaldehyde

: 343332-78-5
C₅₀H₇₂N₈O₁₂Si

Guidance literature:: Multi-step reaction with 5 steps

1.1: 88 percent / DMAP; Et₃N / tetrahydrofuran / 18 h / 20 °C

2.1: NH₂OH / methanol / 3 h / Heating

2.2: trifluoroacetic anhydride; Et₃N / tetrahydrofuran / 5 h / Heating

3.1: CH₂Cl₂ / 5 h / 0 - 20 °C

3.2: NH₃ / methanol / 2 h / 20 °C

3.3: DMAP; Et₃N / tetrahydrofuran / 22 h / 20 °C

4.1: N-methylmorpholine N-oxide; OsO₄ / acetone; H₂O / 23 h / 20 °C

4.2: NaIO₄ / CH₂Cl₂; H₂O / 36 h / 20 °C

5.1: 72 percent / diisopropylethylamine; NaB(OAc)3H / 1,2-dichloro-ethane / 16 h / 20 °C

With dmap; osmium(VIII) oxide; hydroxylamine; sodium tris(acetoxy)borohydride; 4-methylmorpholine N-oxide; triethylamine; N-ethyl-N,N-diisopropylamine; In tetrahydrofuran; methanol; dichloromethane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ja005886l

Reference yield:

: 343332-62-7
(4-allylamino-6-benzyloxy-5-formyl-pyrimidin-2-yl)-methyl-carbamic acid tert-butyl ester

: 343332-78-5
C₅₀H₇₂N₈O₁₂Si

Guidance literature:: Multi-step reaction with 4 steps

1.1: NH₂OH / methanol / 3 h / Heating

1.2: trifluoroacetic anhydride; Et₃N / tetrahydrofuran / 5 h / Heating

2.1: CH₂Cl₂ / 5 h / 0 - 20 °C

2.2: NH₃ / methanol / 2 h / 20 °C

2.3: DMAP; Et₃N / tetrahydrofuran / 22 h / 20 °C

3.1: N-methylmorpholine N-oxide; OsO₄ / acetone; H₂O / 23 h / 20 °C

3.2: NaIO₄ / CH₂Cl₂; H₂O / 36 h / 20 °C

4.1: 72 percent / diisopropylethylamine; NaB(OAc)3H / 1,2-dichloro-ethane / 16 h / 20 °C

With osmium(VIII) oxide; hydroxylamine; sodium tris(acetoxy)borohydride; 4-methylmorpholine N-oxide; N-ethyl-N,N-diisopropylamine; In methanol; dichloromethane; water; 1,2-dichloro-ethane; acetone;
DOI:10.1021/ja005886l