diphenethyl disulfide

Base Information

• Chemical Name: diphenethyl disulfide
• CAS No.: 27846-22-6
• Molecular Formula: C₁₆H₁₈S₂
• Molecular Weight: 274.451
• Mol file: 27846-22-6.mol

Synonyms:diphenethyl disulfide

Chemical Property of diphenethyl disulfide

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of diphenethyl disulfide

There total 28 articles about diphenethyl disulfide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-mercaptophenylethane (4410-99-5) + toluene-p-sulfonyl bromide (1950-69-2) → diphenethyl disulfide (27846-22-6) + S-phenethyl 4-methylbenzenesulfonothioate (53603-17-1)

Guidance literature:

With triethylamine; In tetrachloromethane; at 0 ℃; for 1h; Yields of byproduct given;

Reference yield: 94.0%

C20H20OS → diphenethyl disulfide (27846-22-6)

Guidance literature:

With 2,3-dicyano-5,6-dichloro-p-benzoquinone; In aq. phosphate buffer; dichloromethane; at 0 - 20 ℃; for 29.5h;

Reference yield: 92.0%

Burgess Reagent (29684-56-8) + 2-mercaptophenylethane (4410-99-5) → triethylammonium methylcarboxysulfaminate + diphenethyl disulfide (27846-22-6)

Guidance literature:

In benzene; at 20 ℃;

DOI:10.1021/jo070099t

upstream raw materials:

2-mercaptophenylethane

n-butyllithium

methyl(phenethyl)sulfane

<2-(ethylthio)ethyl>benzene

Downstream raw materials:

2-phenetyl sulfinyl chloride

S-phenethyl 2-phenylethane-1-sulfonothioate

2-(2-phenyl-ethanesulfinyl)-isoindole-1,3-dione

C₁₅H₂₄N₂O₃S

Refernces

• 1、 Spiliopoulou, Nikoleta,Kokotos, Christoforos G.. "Photochemical metal-free aerobic oxidation of thiols to disulfides". supporting information. p. 546 - 551. Retrieved 2021/01/28.
• 2、 Soleiman-Beigi, Mohammad,Yavari, Issa,Sadeghizadeh, Fatemeh. "A rapid, efficient and green procedure for transformation of alkyl halides/ tosylates to organochalcogens in water". . p. 41 - 44. Retrieved 2017/09/25.