5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE

Base Information

Chemical Name:5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE
CAS No.:13906-26-8
Molecular Formula:C15H8 Cl N3 O
Molecular Weight:281.701
Hs Code.:2914700090
Mol file:13906-26-8.mol

Synonyms:5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE;AKOS BBS-00000675

Suppliers and Price of 5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Matrix Scientific
5-Chloro-6,6a,12-triaza-benzo[a]anthracen-7-one
1g
$ 378.00

American Custom Chemicals Corporation
5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE 95.00%
500MG
$ 772.70

AK Scientific
5-Chloro-6,6a,12-triaza-benzo[a]anthracen-7-one
1g
$ 560.00

Total 4 raw suppliers

Chemical Property of 5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE

Chemical Property:

Boiling Point:487.0±28.0 °C(Predicted)
PKA:0.08±0.20(Predicted)
PSA：47.26000
Density:1.50±0.1 g/cm3(Predicted)
LogP:3.04930

Purity/Quality:

98%min ^*data from raw suppliers

5-Chloro-6,6a,12-triaza-benzo[a]anthracen-7-one ^*data from reagent suppliers

Safty Information:

Pictogram(s):
Hazard Codes:Xi

MSDS Files:: SDS file from LookChem

Useful:

Technology Process of 5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE

There total 8 articles about 5-CHLORO-6,6A,12-TRIAZA-BENZO[A]ANTHRACEN-7-ONE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 62.6%

: 13906-27-9
phthalazino<1,2-c>quinazoline-2,12-dione

: 13906-26-8
5-chloro-8H-phthalazino[1,2-b]quinazolin-8-one

Guidance literature:: With trichlorophosphate; for 5h; Reflux;
DOI:10.3184/174751917X14815427219167

Reference yield:

: 85-44-9
phthalic anhydride

: 1904-58-1
anthranilic acid hydrazide

: 13906-26-8
5-chloro-8H-phthalazino[1,2-b]quinazolin-8-one

Guidance literature:: phthalic anhydride; anthranilic acid hydrazide; In ethylene glycol; at 135 ℃; for 3h;

With trichlorophosphate; In ethylene glycol; at 120 ℃; for 6h;

Reference yield:

: 118-92-3,159201-01-1,50816-84-7,80206-34-4,104809-47-4
anthranilic acid

: 13906-26-8
5-chloro-8H-phthalazino[1,2-b]quinazolin-8-one

Guidance literature:: Multi-step reaction with 3 steps

1.1: bis(trichloromethyl) carbonate / tetrahydrofuran / 10 h / 20 °C / Cooling with ice

1.2: 3.5 h / 105 °C / Inert atmosphere

2.1: ethylene glycol / 2 h / 150 °C / Reflux; Inert atmosphere

3.1: trichlorophosphate / 6 h / 90 °C / Inert atmosphere

With bis(trichloromethyl) carbonate; trichlorophosphate; In tetrahydrofuran; ethylene glycol;