C₂₅H₂₂ClN

Base Information

• Chemical Name: C₂₅H₂₂ClN
• CAS No.: 1235886-42-6
• Molecular Formula: C₂₅H₂₂ClN
• Molecular Weight: 371.909
• Mol file: 1235886-42-6.mol

Synonyms:C₂₅H₂₂ClN

Chemical Property of C₂₅H₂₂ClN

Chemical Property:

Purity/Quality:

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

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Technology Process of C₂₅H₂₂ClN

There total 1 articles about C₂₅H₂₂ClN which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 67.0%

1-styrenyloxytrimethylsilane (13735-81-4) + 1,3-diphenylprop-2-yn-1-yl acetate (93321-44-9) + chloroethylamine (689-98-5) → C25H22ClN (1235886-42-6)

Guidance literature:

1-styrenyloxytrimethylsilane; 1,3-diphenylprop-2-yn-1-yl acetate; With zinc(II) chloride; In chlorobenzene; at 75 ℃; for 0.3h;

chloroethylamine; In chlorobenzene; Reflux;

DOI:10.1039/c003885g

Reference yield: 61.0%

C25H22ClN (1235886-42-6) → 2-benzyl-3,5-diphenyl-1H-pyrrole (1235886-43-7)

Guidance literature:

C₂₅H₂₂ClN; With sodium hydride; In acetonitrile; mineral oil; at 50 ℃; for 2h; Inert atmosphere;

With hydrogenchloride; In water; acetonitrile; mineral oil; for 6h;

With sodium acetate; In water; acetonitrile; mineral oil; for 0.5h; Reflux;

DOI:10.1039/c003885g

upstream raw materials:

1-styrenyloxytrimethylsilane

1,3-diphenylprop-2-yn-1-yl acetate

chloroethylamine

Downstream raw materials:

2-benzyl-3,5-diphenyl-1H-pyrrole