2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

Base Information

Chemical Name:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride
CAS No.:81440-83-7
Molecular Formula:C₁₂H₁₈INO₃S*ClH
Molecular Weight:419.711
Hs Code.:

Synonyms:2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

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Chemical Property of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

Chemical Property:

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Technology Process of 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

There total 3 articles about 2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: Methanesulfonic acid 2-(tert-butoxycarbonylamino-methyl)-4-tert-butyl-6-iodo-phenyl ester

: 81440-83-7
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

Guidance literature:: With hydrogenchloride; In ethanol; at 20 - 25 ℃; for 3h; Yield given;
DOI:10.1021/jm00348a024

Reference yield:

: 58456-91-0
2-aminomethyl-4-tert-butyl-6-iodophenol

: 81440-83-7
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

Guidance literature:: Multi-step reaction with 3 steps

1: 79 percent / Et₃N / tetrahydrofuran; H₂O / 24 h / 60 - 65 °C

2: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

3: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In tetrahydrofuran; ethanol; dichloromethane; water;
DOI:10.1021/jm00348a024

Reference yield:

: 68967-65-7
1,1-dimethylethyl N-<<5-(1,1-dimethylethyl)-2-hydroxy-3-iodophenyl>methyl>carbamate

: 81440-83-7
2-(aminomethyl)-4-(1,1-dimethylethyl)-6-iodophenyl methanesulfonate hydrochloride

Guidance literature:: Multi-step reaction with 2 steps

1: Et₃N / CH₂Cl₂ / 72 h / 20 - 25 °C

2: conc. HCl / ethanol / 3 h / 20 - 25 °C

With hydrogenchloride; triethylamine; In ethanol; dichloromethane;
DOI:10.1021/jm00348a024