Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

Base Information

Chemical Name:Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride
CAS No.:87517-93-9
Molecular Formula:C₂₆H₂₄ClO₂P₂*Cl
Molecular Weight:501.329
Hs Code.:

Synonyms:Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

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Technology Process of Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

There total 1 articles about Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 44.0%

: 14212-98-7
phenyl bis(chloromethyl)phosphinate

: 603-35-0
triphenylphosphine

: 87517-93-9
Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

Guidance literature:: In xylene; at 110 ℃;
DOI:10.1021/jo00172a065

Reference yield:

: 87517-93-9
Phenyl (chloromethyl)(triphenylphosphoniomethyl)phosphinate chloride

: 80991-34-0
(S)-Phenyl (3,4-dioctadecoxybutyl)<(diethoxyphosphinyl)methyl>phosphinate

Guidance literature:: Multi-step reaction with 3 steps

1: 20percent aq. K₂CO₃ / toluene / Ambient temperature

2: 35 percent / toluene / 40 h / 115 °C

3: 53.8 percent / 2) H₂ / 2) 10percent Pd/C / 1) 150 degC, 48 h, 2) THF (1percent EtOH), 50 lb/in², room temp., overnight

With hydrogen; potassium carbonate; palladium on activated charcoal; In toluene;
DOI:10.1021/jo00172a065