trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

Base Information

Chemical Name:trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate
CAS No.:114250-38-3
Molecular Formula:C₂₃H₂₆O₁₀
Molecular Weight:462.453
Hs Code.:

Synonyms:trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

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Chemical Property of trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

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Technology Process of trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

There total 4 articles about trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 2144-45-8
dibenzyl peroxydicarbonate

: 114250-38-3
trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dimethylformamide / 1) 0 deg C, 30 min; 2) 1 h, room temperature

2: 1.) pyridine / 1) CH₂Cl₂, 30 min, room temperature; 2) CH₂Cl₂, 0 deg C, 1 h, room temperature, overnight

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00402a032

Reference yield:

: 114250-44-1
trans-2-(acetyloxy)-1-cyclohexanecarboxylic acid

: 114250-38-3
trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / oxalyl chloride / CH₂Cl₂ / 1) 0 deg C, 30 min; 2) 3 h, room temperature

2: 1.) pyridine / 1) CH₂Cl₂, 30 min, room temperature; 2) CH₂Cl₂, 0 deg C, 1 h, room temperature, overnight

With pyridine; oxalyl dichloride; In dichloromethane;
DOI:10.1021/jm00402a032

Reference yield:

: 5284-32-2
Meldrum's acid sodium salt

: 114250-38-3
trans-5-<<2-(acetyloxy)cyclohexyl>carbonyl>-2,2-dimethyl-4,6-dioxo-1,3-dioxan-5-yl phenylmethyl carbonate

Guidance literature:: Multi-step reaction with 2 steps

1: 81 percent / dimethylformamide / 1) 0 deg C, 30 min; 2) 1 h, room temperature

2: 1.) pyridine / 1) CH₂Cl₂, 30 min, room temperature; 2) CH₂Cl₂, 0 deg C, 1 h, room temperature, overnight

With pyridine; In N,N-dimethyl-formamide;
DOI:10.1021/jm00402a032