Technology Process of N3-(3-chloro-4-(phenylthio)phenyl)-1H-1,2,4-triazole-3,5-diamine
There total 6 articles about N3-(3-chloro-4-(phenylthio)phenyl)-1H-1,2,4-triazole-3,5-diamine which
guide to synthetic route it.
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synthetic route:
- Guidance literature:
-
With
hydrazine;
In
ethanol;
for 1h;
Reflux;
- Guidance literature:
-
Multi-step reaction with 4 steps
1.1: iron; ammonium chloride / water; methanol / 6 h / Reflux
2.1: calcium carbonate / water; dichloromethane / 0.17 h / 0 °C / Inert atmosphere
2.2: 4 h / 0 - 20 °C / Inert atmosphere
3.1: sodium methylate / methanol / 0.25 h / Inert atmosphere
3.2: 1 h / Inert atmosphere
3.3: 20 °C / Inert atmosphere
4.1: hydrazine / ethanol / 1 h / Reflux
With
sodium methylate; iron; ammonium chloride; calcium carbonate; hydrazine;
In
methanol; ethanol; dichloromethane; water;
- Guidance literature:
-
Multi-step reaction with 2 steps
1.1: sodium methylate / methanol / 0.25 h / Inert atmosphere
1.2: 1 h / Inert atmosphere
1.3: 20 °C / Inert atmosphere
2.1: hydrazine / ethanol / 1 h / Reflux
With
sodium methylate; hydrazine;
In
methanol; ethanol;