2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

Base Information

Chemical Name:2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide
CAS No.:1200026-75-0
Molecular Formula:C₁₇H₁₆Cl₂N₈O₄
Molecular Weight:467.271
Hs Code.:

Synonyms:2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

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Chemical Property of 2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

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Technology Process of 2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

There total 1 articles about 2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 68.0%

: 1200026-66-9
ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate

: 1200026-75-0
2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

Guidance literature:: With hydrazine hydrate; In ethanol; for 8h; Reflux;
DOI:10.3390/molecules14072431

Reference yield: 69.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1200026-75-0
2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

: 1200026-93-2
3'-(2-chloroethyl)-5-(4-chlorophenylmethylidene)-3-{[5-mercapto-1,3,4-oxadiazol-2-yl-methyl]amino}-2'-nitro-3,5-dihydro-3'H,4H-2,4'-biimidazol-4-one

Guidance literature:: With potassium hydroxide; In ethanol; for 3h; Reflux;
DOI:10.3390/molecules14072431

Reference yield: 48.0%

: 75-15-0,12122-00-8
carbon disulfide

: 1200026-75-0
2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

: 1200027-03-7
3-{[(4-amino-5-mercapto-4H-1,2,4-triazol-3-yl)methyl]amino}-3'-(2-chloroethyl)-5-(4-chlorophenylmethylidene)-2'-nitro-3',5-dihydro-3'H,4H-2,4'-biimidazol-4-one

Guidance literature:: carbon disulfide; 2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide; In ethanol; for 12h;

With hydrazine hydrate; In water; for 1h; Reflux;
DOI:10.3390/molecules14072431