ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate

Base Information

• Chemical Name: ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate
• CAS No.: 1200026-66-9
• Molecular Formula: C₁₉H₁₈Cl₂N₆O₅
• Molecular Weight: 481.295

Synonyms:ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate

Chemical Property of ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate

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Technology Process of ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate

There total 1 articles about ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 65.0%

C15H12Cl2N6O3 (1200026-30-7) + ethyl bromoacetate (105-36-2) → ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate (1200026-66-9)

Guidance literature:

C₁₅H₁₂Cl₂N₆O₃; With sodium; In ethanol; for 2h; Reflux;

ethyl bromoacetate; In ethanol; for 5h; Reflux;

DOI:10.3390/molecules14072431

Reference yield: 68.0%

ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate (1200026-66-9) → 2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide (1200026-75-0)

Guidance literature:

With hydrazine hydrate; In ethanol; for 8h; Reflux;

DOI:10.3390/molecules14072431

Reference yield: 35.0%

ethyl {[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetate (1200026-66-9) + thiosemicarbazide (79-19-6) → C18H17Cl2N9O4S (1200026-84-1)

Guidance literature:

In ethanol; for 8h; Reflux;

DOI:10.3390/molecules14072431

upstream raw materials:

C₁₅H₁₂Cl₂N₆O₃

ethyl bromoacetate

Downstream raw materials:

2-{[3'-(2-chloroethyl)-4-(4-chlorophenylmethylidene)-2'-nitro-5-oxo-4,5-dihydro-1H,3'H-2,4'-biimidazol-1-yl]-amino}acetohydrazide

C₁₈H₁₇Cl₂N₉O₄S

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