1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

Base Information

Chemical Name:1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol
CAS No.:160835-91-6
Molecular Formula:C₄₄H₄₆O₇
Molecular Weight:686.845
Hs Code.:

Synonyms:1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

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Chemical Property of 1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

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Technology Process of 1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

There total 4 articles about 1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 3396-11-0
cesium acetate

: 160835-90-5
1D-1,3,4,5,6-penta-O-benzyl-2-O-methylsulfonyl-5-C-methyl-1,2,3,5/4,6-cyclohehanehexol

: 160835-91-6
1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

Guidance literature:: In N,N-dimethyl-formamide; at 80 ℃; for 12h;
DOI:10.1246/bcsj.67.1633

Reference yield:

: 100-39-0
benzyl bromide

: 160835-91-6
1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Bu₂SnO / 1.) toluene, reflux, 2 h, 2.) toluene, DMF, 80 deg C, 3 h

2: 97 percent / pyridine / 24 h / 0 °C / Irradiation

3: 93 percent / dimethylformamide / 12 h / 80 °C

With pyridine; di(n-butyl)tin oxide; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.67.1633

Reference yield:

: (3S,4R,5R,6S)-3,4,5,6-Tetrakis-benzyloxy-4-methyl-cyclohexane-1,2-diol

: 160835-91-6
1D-1-O-acetyl-2,3,4,5,6-penta-O-benzyl-4-C-methyl-1,3,5/2,4,6-cyclohehanehexol

Guidance literature:: Multi-step reaction with 3 steps

1: 1.) Bu₂SnO / 1.) toluene, reflux, 2 h, 2.) toluene, DMF, 80 deg C, 3 h

2: 97 percent / pyridine / 24 h / 0 °C / Irradiation

3: 93 percent / dimethylformamide / 12 h / 80 °C

With pyridine; di(n-butyl)tin oxide; In N,N-dimethyl-formamide;
DOI:10.1246/bcsj.67.1633