methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

Base Information

Chemical Name:methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside
CAS No.:352547-27-4
Molecular Formula:C₂₄H₃₁NO₇
Molecular Weight:445.513
Hs Code.:

Synonyms:methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

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Chemical Property of methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

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Technology Process of methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

There total 3 articles about methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 59.0%

: 352547-26-3
methyl 2-acetamido-3,4-di-O-benzyl-2,7-dideoxy-7-(phenydimethylsilyl)-L-glycero-β-D-gluco-heptopyranoside

: 352547-27-4
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

Guidance literature:: With sodium acetate; potassium bromide; In acetic acid; at 0 ℃; for 2h;
DOI:10.1016/S0008-6215(01)00078-7

Reference yield:

: 69892-53-1
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 352547-27-4
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

Guidance literature:: Multi-step reaction with 3 steps

1: 69 percent / Dess-Martin periodinane / CH₂Cl₂ / 120 h / 32 °C

2: 63 percent / tetrahydrofuran / 2 h / -20 °C

3: 59 percent / KBr; NaOAc / acetic acid / 2 h / 0 °C

With sodium acetate; Dess-Martin periodane; potassium bromide; In tetrahydrofuran; dichloromethane; acetic acid;
DOI:10.1016/S0008-6215(01)00078-7

Reference yield:

: 213487-09-3
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

: 352547-27-4
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-L-glycero-β-D-gluco-heptopyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 63 percent / tetrahydrofuran / 2 h / -20 °C

2: 59 percent / KBr; NaOAc / acetic acid / 2 h / 0 °C

With sodium acetate; potassium bromide; In tetrahydrofuran; acetic acid;
DOI:10.1016/S0008-6215(01)00078-7