methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

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Chemical Name:methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside
CAS No.:213487-09-3
Molecular Formula:C₂₃H₂₇NO₆
Molecular Weight:413.47
Hs Code.:

Synonyms:methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

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Chemical Property of methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

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Technology Process of methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

There total 2 articles about methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 69.0%

: 69892-53-1
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-glucopyranoside

: 213487-09-3
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

Guidance literature:: With Dess-Martin periodane; In dichloromethane; at 32 ℃; for 120h;
DOI:10.1016/S0008-6215(01)00078-7

Reference yield:

: 69892-51-9
Methyl-2-acetamido-3,4-di-O-benzyl-6-O-trityl-2-deoxy-β-D-glucopyranosid

: 213487-09-3
methyl 2-acetamido-3,4-di-O-benzyl-2-deoxy-β-D-gluco-hexodialdo-1,5-pyranoside

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / HBr / acetic acid; CH₂Cl₂ / 0.05 h / 5 °C

2: 1.) (COCl)2, DMSO, 2.) Et₃N / 1.) CH₂Cl₂, -78 deg C, 15 min, 2.) -78 deg C to room temperature, 30 min

With oxalyl dichloride; hydrogen bromide; dimethyl sulfoxide; triethylamine; In dichloromethane; acetic acid;
DOI:10.1021/jo980781a