N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

Base Information

Chemical Name:N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide
CAS No.:260782-38-5
Molecular Formula:C₂₀H₂₇NO₇
Molecular Weight:393.437
Hs Code.:

Synonyms:N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

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Technology Process of N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

There total 2 articles about N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 85006-25-3
N,N-di(tert-butoxycarbonyl)hydroxylamine

: 66696-84-2
5-(1-hydroxy-2-phenylethylidene)-2,2-dimethyl-1,3-dioxane-4,6-dione

: 260782-38-5
N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

Guidance literature:: In toluene; at 65 ℃; for 16h;
DOI:10.1021/jo991409d

Reference yield:

: 103-80-0
phenylacetyl chloride

: 260782-38-5
N-(tert-butoxycarbonyl)-N-(tert-butoxycarbonyloxy)-3-oxo-4-phenylbutyramide

Guidance literature:: Multi-step reaction with 2 steps

1: 100 percent / pyridine / CH₂Cl₂ / 0 - 20 °C

2: 75 percent / toluene / 16 h / 65 °C

With pyridine; In dichloromethane; toluene; 1: Acylation / 2: Substitution;
DOI:10.1021/jo991409d