3-phenyl-3-iminothiopropionamide

Base Information

• Chemical Name: 3-phenyl-3-iminothiopropionamide
• CAS No.: 16187-91-0
• Molecular Formula: C₉H₁₀N₂S
• Molecular Weight: 178.258

Synonyms:3-phenyl-3-iminothiopropionamide

Chemical Property of 3-phenyl-3-iminothiopropionamide

Chemical Property:

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Technology Process of 3-phenyl-3-iminothiopropionamide

There total 3 articles about 3-phenyl-3-iminothiopropionamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 26.0%

3-amino-3-phenylacrylonitrile (1823-99-0,17196-74-6,60375-56-6) → 3-phenyl-3-iminothiopropionamide (16187-91-0)

Guidance literature:

With diphenylphosphinodithioic acid; In isopropyl alcohol; at 40 ℃; for 20h;

DOI:10.1021/ja00085a008

Reference yield:

β-imino-β-phenylpropionitrile (16187-90-9) → 3-phenyl-3-iminothiopropionamide (16187-91-0)

Guidance literature:

With potassium hydroxide; hydrogen sulfide; In dichloromethane;

Reference yield:

→ 3-phenyl-3-iminothiopropionamide (16187-91-0)

Guidance literature:

β-Imino-β-phenyl-propionitril in CH2Cl2 m. KOH u. H2S (80grad; Rohr);

upstream raw materials:

3-amino-3-phenylacrylonitrile

β-imino-β-phenylpropionitrile

Downstream raw materials:

S-(2-nitro-phenyl)-N-(3-phenyl-isothiazol-5-yl)-thiohydroxylamine

5-chloro-3-phenyl-isothiazole

N-(3-phenyl-isothiazol-5-yl)-formamide

5-bromo-3-phenyl-isothiazole

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