2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

Base Information

Chemical Name:2-acetyl-5-methoxyphenyl thiophene-2-carboxylate
CAS No.:92254-80-3
Molecular Formula:C₁₄H₁₂O₄S
Molecular Weight:276.313
Hs Code.:

Synonyms:2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

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Chemical Property of 2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

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Technology Process of 2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

There total 1 articles about 2-acetyl-5-methoxyphenyl thiophene-2-carboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 89.0%

: 5271-67-0
2-Thiophenecarbonyl chloride

: 552-41-0
1-(2-hydroxy-4-methoxyphenyl)ethanone

: 92254-80-3
2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

Guidance literature:: With pyridine; at 25 ℃; for 5h;
DOI:10.1002/ejoc.201100435

Reference yield: 71.0%

: 92254-80-3
2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

: 92254-77-8
1-(2-hydroxy-4-methoxyphenyl)-3-(thiophen-2-yl)propane-1,3-dione

Guidance literature:: With potassium carbonate; In pyridine; at 75 ℃;
DOI:10.1002/ejoc.201100435

Reference yield:

: 92254-80-3
2-acetyl-5-methoxyphenyl thiophene-2-carboxylate

: 1333334-77-2
5-methoxy-2-[3-oxo-3-(thiophen-2-yl)propanoyl]phenyl acetate

Guidance literature:: Multi-step reaction with 2 steps

1: potassium carbonate / pyridine / 75 °C

2: pyridine / 2 h / 25 °C

With pyridine; potassium carbonate; In pyridine; 1: Baker-Venkataraman rearrangement;
DOI:10.1002/ejoc.201100435