1-(1-Ethoxyethoxy)-2-methylbutane

Base Information

Chemical Name:1-(1-Ethoxyethoxy)-2-methylbutane
CAS No.:13602-09-0
Molecular Formula:C₉H₂₀O₂
Molecular Weight:160.257
Hs Code.:
DSSTox Substance ID:DTXSID00699670
Mol file:13602-09-0.mol

Synonyms:1-(1-Ethoxyethoxy)-2-methylbutane;13602-09-0;ethoxy-2-methylbut oxyethane;DTXSID00699670;Butane, 1-(1-ethoxyethoxy)-2-methyl-;1-ETHOXY-1-(2-METHYLBUTOXY)ETHANE

Suppliers and Price of 1-(1-Ethoxyethoxy)-2-methylbutane

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 6 raw suppliers

Chemical Property of 1-(1-Ethoxyethoxy)-2-methylbutane

Chemical Property:

Boiling Point:167.5±8.0 °C(Predicted)
PSA：18.46000
Density:0.840±0.06 g/cm3(Predicted)
LogP:2.43160
XLogP3:2.5
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:6
Exact Mass:160.146329876
Heavy Atom Count:11
Complexity:83.6

Purity/Quality:: 98%min ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:CCC(C)COC(C)OCC

Technology Process of 1-(1-Ethoxyethoxy)-2-methylbutane

There total 5 articles about 1-(1-Ethoxyethoxy)-2-methylbutane which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 187083-84-7
(2R)-(+)-3-(1'-ethoxyethoxy)-2-methylpropanol

: 13602-09-0,115166-86-4,115166-89-7
Acetaldehyde O-ethyl O'-(R)-2-methylpropyl acetal

Guidance literature:: Multi-step reaction with 2 steps

1: triethylamine / CH₂Cl₂

2: 1.) ether, 0 deg C; 2.) ether, 0 deg C

With triethylamine; In dichloromethane;

Reference yield:

: 104199-85-1,115166-84-2,115166-87-5,142459-19-6,142459-20-9
Methyl (S)-(+)-3-(1-ethoxyethoxy)-2-methylpropanoate

: 13602-09-0,115166-86-4,115166-89-7
Acetaldehyde O-ethyl O'-(R)-2-methylpropyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: 95 percent / LiAlH₄ / diethyl ether / 0.5 h / -78 °C

2: 91 percent / Et₃N / CH₂Cl₂ / 1 h / 25 °C

3: 1.) CuI / 1.) Et₂O, 0 deg C, 2.) 0 deg C, 1 h

With copper(l) iodide; lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;
DOI:10.1055/s-1988-27458

Reference yield:

: (S)-3-(1-Ethoxy-ethoxy)-2-methyl-propionic acid methyl ester

: 13602-09-0,115166-86-4,115166-89-7
Acetaldehyde O-ethyl O'-(R)-2-methylpropyl acetal

Guidance literature:: Multi-step reaction with 3 steps

1: lithium aluminium hydride / diethyl ether / -78 °C

2: triethylamine / CH₂Cl₂

3: 1.) ether, 0 deg C; 2.) ether, 0 deg C

With lithium aluminium tetrahydride; triethylamine; In diethyl ether; dichloromethane;