(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

Base Information

Chemical Name:(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine
CAS No.:1353547-85-9
Molecular Formula:C₂₃H₃₀N₂O₆S
Molecular Weight:462.567
Hs Code.:

Synonyms:(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

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Chemical Property of (E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

Chemical Property:

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Technology Process of (E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

There total 6 articles about (E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 110-89-4
piperidine

: 830-79-5
2,4,6-trimethoxybenzaldehyde

: 1353548-03-4
2-(((5-methoxy-6-nitropyridin-2-yl)methyl)sulfonyl)acetic acid

: 1353547-85-9
(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

Guidance literature:: With pyridine; In toluene; for 5h; Reflux;

Reference yield:

: 15128-90-2
6-methyl-2-nitropyridin-3-ol

: 1353547-85-9
(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

Guidance literature:: Multi-step reaction with 6 steps

1.1: potassium carbonate / dimethyl sulfoxide / 24 h / 20 °C

2.1: dibenzoyl peroxide; N-Bromosuccinimide / tetrachloromethane / 56 h / Inert atmosphere; Reflux

3.1: potassium carbonate / methanol / 10 h / 20 °C

4.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

5.1: water; sodium carbonate / methanol / 10 h / 20 °C

5.2: pH 2

6.1: pyridine / toluene / 5 h / Reflux

With pyridine; N-Bromosuccinimide; water; dihydrogen peroxide; sodium carbonate; potassium carbonate; acetic acid; dibenzoyl peroxide; In methanol; tetrachloromethane; dimethyl sulfoxide; toluene;

Reference yield:

: 1353547-96-2
methyl 2-(((5-methoxy-6-nitropyridin-2-yl)methyl)thio)acetate

: 1353547-85-9
(E)-3-methoxy-2-(piperidin-1-yl)-6-((2,4,6-trimethoxystyrylsulfonyl)methyl)pyridine

Guidance literature:: Multi-step reaction with 3 steps

1.1: dihydrogen peroxide; acetic acid / 7 h / 50 °C

2.1: water; sodium carbonate / methanol / 10 h / 20 °C

2.2: pH 2

3.1: pyridine / toluene / 5 h / Reflux

With pyridine; water; dihydrogen peroxide; sodium carbonate; acetic acid; In methanol; toluene;