Pyrimidine, 2-(1H-tetrazol-5-yl)- (8CI,9CI)

Base Information

• Chemical Name: Pyrimidine, 2-(1H-tetrazol-5-yl)- (8CI,9CI)
• CAS No.: 13600-33-4
• Molecular Formula: C5H4 N6
• Molecular Weight: 148.12546
• Hs Code.: 2933990090
• Mol file: 13600-33-4.mol

Synonyms:Pyrimidine,2-(1H-tetrazol-5-yl)- (8CI,9CI); Pyrimidine, 2-tetrazol-5-yl- (7CI);2-(1H-Tetrazol-5-yl)pyrimidine; 5-(2-Pyrimidinyl)tetrazole;5-(2-Pyrimidyl)tetrazole

Chemical Property of Pyrimidine, 2-(1H-tetrazol-5-yl)- (8CI,9CI)

Chemical Property:

• Melting Point: 233 °C
• Boiling Point: 443.8±28.0 °C(Predicted)
• PKA: 2.84±0.10(Predicted)
• PSA: 80.24000
• Density: 1.493±0.06 g/cm3(Predicted)
• LogP: -0.34330

Purity/Quality:

99.0% ^*data from raw suppliers

2-(1H-Tetrazol-5-yl)pyrimidine ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of Pyrimidine, 2-(1H-tetrazol-5-yl)- (8CI,9CI)

There total 3 articles about Pyrimidine, 2-(1H-tetrazol-5-yl)- (8CI,9CI) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 95.0%

2-cyanopyrimidine (14080-23-0) → 2-(1H-tetrazol-5-yl)pyrimidine (13600-33-4)

Guidance literature:

With sodium azide; betaine; zinc(II) chloride; In water; at 20 ℃; for 20h;

Reference yield:

2-cyanopyrimidyl → 2-(1H-tetrazol-5-yl)pyrimidine (13600-33-4)

Guidance literature:

With sodium azide; triethylamine hydrochloride; In toluene;

DOI:10.1002/zaac.201500134

Reference yield:

→ 2-(1H-tetrazol-5-yl)pyrimidine (13600-33-4)

Guidance literature:

2-Cyan-pyrimidin, NaN3, Essigsaeure, in Propanol-(2), (Druck, 150gradC, 105 Std.);

upstream raw materials:

2-cyanopyrimidine