tributyl benzene-1,3,5-tricarboxylate

Base Information

Chemical Name:tributyl benzene-1,3,5-tricarboxylate
CAS No.:104564-69-4
Molecular Formula:C₂₁H₃₀O₆
Molecular Weight:378.466
Hs Code.:

Synonyms:tributyl benzene-1,3,5-tricarboxylate

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Chemical Property of tributyl benzene-1,3,5-tricarboxylate

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Technology Process of tributyl benzene-1,3,5-tricarboxylate

There total 3 articles about tributyl benzene-1,3,5-tricarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 94.0%

: 626-39-1
1,3,5-trisbromobenzene

: 201230-82-2
carbon monoxide

: 71-36-3
butan-1-ol

: 104564-69-4
tributyl benzene-1,3,5-tricarboxylate

Guidance literature:: 1,3,5-trisbromobenzene; butan-1-ol; With palladium diacetate; 2,2'-bis-(diphenylphosphino)-1,1'-binaphthyl; N-ethyl-N,N-diisopropylamine; In 5,5-dimethyl-1,3-cyclohexadiene; at 20 ℃; for 1h; Inert atmosphere; Glovebox;

carbon monoxide; In 5,5-dimethyl-1,3-cyclohexadiene; at 120 - 140 ℃; for 12h; under 22801.5 Torr; Autoclave;
DOI:10.1055/a-1587-8859