methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

Base Information

Chemical Name:methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate
CAS No.:317819-92-4
Molecular Formula:C₁₈H₃₁NO₅
Molecular Weight:341.448
Hs Code.:

Synonyms:methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

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Chemical Property of methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

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Technology Process of methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

There total 2 articles about methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 24424-99-5
di-tert-butyl dicarbonate

: 317819-93-5
methyl 4-[(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

: 317819-92-4
methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

Guidance literature:: With triethylamine; In water; acetonitrile; at 20 ℃; for 20h;
DOI:10.1021/jm901154c

Reference yield:

: 24424-99-5
di-tert-butyl dicarbonate

: 317819-92-4
methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

Guidance literature:: With triethylamine;

Reference yield: 48.0%

: 256453-94-8
2-(2-methylphenylamino)-6-benzoxazolylacetic acid

: EDC(HCl

: 317819-92-4
methyl 4-[N-(tert-butoxycarbonyl)-(2S)-pyrrolidinylmethoxy]cyclohexanecarboxylate

: ethyl acetate n-hexane

: 77-92-9,906507-37-7
citric acid

: 441769-13-7
methyl 4-(1-(2-(2-methylphenylamino)-6-benzoxazolylacetyl)-(2S)-pyrrolidinylmethoxy)cyclohexanecarboxylate

Guidance literature:: With sodium hydrogencarbonate; benzotriazol-1-ol; triethylamine; In (2S)-N-methyl-1-phenylpropan-2-amine hydrate; dichloromethane;