6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

Base Information

Chemical Name:6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on
CAS No.:60055-35-8
Molecular Formula:C₂₀H₂₀N₂O₅
Molecular Weight:368.389
Hs Code.:

Synonyms:6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

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Chemical Property of 6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

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Technology Process of 6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

There total 4 articles about 6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 108-24-7
acetic anhydride

: 60055-34-7
2-Benzyloxy-1-nitro-8,9-dihydro-7H-benzocycloheptene-5,6-dione 6-oxime

: 60055-35-8
6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

Guidance literature:: With hydrogen; nickel; In acetic acid; under 760 Torr; Ambient temperature;

Reference yield:

: 60055-30-3
2-Hydroxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

: 60055-35-8
6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

Guidance literature:: Multi-step reaction with 3 steps

1: potassium carbonate; potassium iodide / methanol / Heating

2: hydrogenchloride; ethanol; isopentyl nitrite / tetrahydrofuran; diethyl ether / 0 °C

3: hydrogen / nickel / acetic acid / 760 Torr / Ambient temperature

With hydrogenchloride; ethanol; hydrogen; potassium carbonate; potassium iodide; isopentyl nitrite; nickel; In tetrahydrofuran; methanol; diethyl ether; acetic acid;

Reference yield:

: 60055-31-4
2-Benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

: 60055-35-8
6-Acetamido-2-benzyloxy-1-nitro-6,7,8,9-tetrahydro-5H-benzocyclohepten-5-on

Guidance literature:: Multi-step reaction with 2 steps

1: hydrogenchloride; ethanol; isopentyl nitrite / tetrahydrofuran; diethyl ether / 0 °C

2: hydrogen / nickel / acetic acid / 760 Torr / Ambient temperature

With hydrogenchloride; ethanol; hydrogen; isopentyl nitrite; nickel; In tetrahydrofuran; diethyl ether; acetic acid;