C₁₆H₁₄⁽²⁾H₂N₂

Base Information

Chemical Name:C₁₆H₁₄⁽²⁾H₂N₂
CAS No.:1361111-06-9
Molecular Formula:C₁₆H₁₆N₂
Molecular Weight:238.301
Hs Code.:

C<sub>16</sub>H<sub>14</sub><sup>(2)</sup>H<sub>2</sub>N<sub>2</sub>

Synonyms:C₁₆H₁₄⁽²⁾H₂N₂

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₁₆H₁₄⁽²⁾H₂N₂

Chemical Property:

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Technology Process of C₁₆H₁₄⁽²⁾H₂N₂

There total 4 articles about C₁₆H₁₄⁽²⁾H₂N₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1361110-35-1
methyl 3-(benzylamino)-2,2-dideutero-3-(4-bromophenyl)propanoate

: 1361111-06-9
C₁₆H₁₄⁽²⁾H₂N₂

Guidance literature:: Multi-step reaction with 3 steps

1.1: palladium on activated charcoal; ammonium formate

2.1: potassium carbonate / methanol / 20 °C

3.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

3.2: 4 h / -78 °C / Inert atmosphere

3.3: Saturated solution

With palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 27046-29-3
N-(4-bromobenzylidene)benzylamine

: 1361111-06-9
C₁₆H₁₄⁽²⁾H₂N₂

Guidance literature:: Multi-step reaction with 5 steps

1.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

1.2: 4 h / -78 °C / Inert atmosphere

1.3: Saturated solution

2.1: sulfuric acid / 0 °C / Reflux

3.1: palladium on activated charcoal; ammonium formate

4.1: potassium carbonate / methanol / 20 °C

5.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

5.2: 4 h / -78 °C / Inert atmosphere

5.3: Saturated solution

With sulfuric acid; palladium on activated charcoal; ammonium formate; potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004

Reference yield:

: 100-52-7
benzaldehyde

: 1361111-06-9
C₁₆H₁₄⁽²⁾H₂N₂

Guidance literature:: Multi-step reaction with 2 steps

1.1: potassium carbonate / methanol / 20 °C

2.1: lithium diisopropyl amide / tetrahydrofuran / 0.5 h / -78 °C / Inert atmosphere

2.2: 4 h / -78 °C / Inert atmosphere

2.3: Saturated solution

With potassium carbonate; lithium diisopropyl amide; In tetrahydrofuran; methanol;
DOI:10.1016/j.tetlet.2012.01.004