(2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

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Chemical Name:(2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid
CAS No.:1155870-72-6
Molecular Formula:C₂₆H₃₀N₂O₆
Molecular Weight:466.534
Hs Code.:

Synonyms:(2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

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Chemical Property of (2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

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Technology Process of (2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

There total 1 articles about (2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 1155870-71-5
tert-butyl (6R)-6-({5-[(1E)-3-(allyloxy)-3-oxoprop-1-en-1-yl]-6-phenylfuro[2,3-d]pyrimidin-4-yl}oxy)heptanoate

: 1155870-72-6
(2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

Guidance literature:: With morpholine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; In tetrahydrofuran; at 20 ℃; for 3h; Inert atmosphere;

Reference yield: 72.6%

: 1155870-72-6
(2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid

: 75-04-7,85404-22-4
ethylamine

: 1155870-75-9
tert-Butyl (6R)-6-({5-[(1E)-3-(ethylamino)-3-oxoprop-1-en-1-yl]-6-phenylfuro[2,3-d]pyrimidin-4-yl}oxy)heptanoate

Guidance literature:: (2E)-3-(4-{[(1R)-6-tert-butoxy-1-methyl-6-oxohexyl]oxy}-6-phenylfuro[2,3-d]pyrimidin-5-yl)acrylic acid; With HATU; In N,N-dimethyl-formamide; at 0 ℃; for 0.166667h;

ethylamine; With N-ethyl-N,N-diisopropylamine; In methanol; N,N-dimethyl-formamide; at 20 ℃;