C₄₃H₆₁N₃O₁₀Si₂

Base Information

Chemical Name:C₄₃H₆₁N₃O₁₀Si₂
CAS No.:182201-57-6
Molecular Formula:C₄₃H₆₁N₃O₁₀Si₂
Molecular Weight:836.142
Hs Code.:

C<sub>43</sub>H<sub>61</sub>N<sub>3</sub>O<sub>10</sub>Si<sub>2</sub>

Synonyms:C₄₃H₆₁N₃O₁₀Si₂

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Chemical Property of C₄₃H₆₁N₃O₁₀Si₂

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Technology Process of C₄₃H₆₁N₃O₁₀Si₂

There total 20 articles about C₄₃H₆₁N₃O₁₀Si₂ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 87.0%

: 106-95-6
allyl bromide

: 182201-65-6
C₄₀H₅₇N₃O₁₀Si₂

: 182201-57-6
C₄₃H₆₁N₃O₁₀Si₂

Guidance literature:: With caesium carbonate; In N,N-dimethyl-formamide; at 23 ℃; for 1h;
DOI:10.1021/ja962480t

Reference yield:

: 111726-43-3
3,4-(methylenedioxy)phenyl methoxymethyl ether

: 182201-57-6
C₄₃H₆₁N₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 14 steps

1: 1.) BuLi, tetramethylethylene diamine / 1.) hexane, 0 deg C, 4 h, 2.) hexane, from -78 deg C to 23 deg C, 15 min

2: 1.) BuLi / 1.) THF, -30 deg C, 13 h

3: CH₃SO₃H / CH₂Cl₂ / 0 °C

4: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 23 deg C, 40 min

5: 99 percent / piperidine, acetic acid / benzene / 18 h / 23 °C

6: 94 percent / Et₃N, HCOOH, Pd(PPh₃)4 / 4 h / 23 °C

7: (PhO)2P(O)N₃, Et₃N, 4 Angstroem molecular sieves / toluene / 2 h / 70 °C

8: 1 h / 23 °C

9: 97 percent / H₂, Rh<(COD)-(R,R)-DIPAMP>(+)*BF₄(-) / 16 h / 23 °C / 2280 Torr

10: BF₃*Et₂O, H₂O / CH₂Cl₂ / 0.17 h / 0 °C

11: BF₃*Et₂O, 4 Angstroem molecular sieves / CH₂Cl₂ / 18 h / 23 °C

12: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h / 23 °C / 760 Torr

13: 61 percent / HOAc / 18 h / 23 °C

14: 87 percent / Cs₂CO₃ / dimethylformamide / 1 h / 23 °C

With piperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; methanesulfonic acid; N,N,N,N,-tetramethylethylenediamine; Rh<(COD)-(R,R)-DIPAMP>(+)*BF4(-); 4 A molecular sieve; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; water; hydrogen; sodium hydride; caesium carbonate; acetic acid; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/ja962480t

Reference yield:

: 187040-02-4
5-methoxy methoxy-4-methyl benzo[d][1,3]dioxole

: 182201-57-6
C₄₃H₆₁N₃O₁₀Si₂

Guidance literature:: Multi-step reaction with 13 steps

1: 1.) BuLi / 1.) THF, -30 deg C, 13 h

2: CH₃SO₃H / CH₂Cl₂ / 0 °C

3: 1.) NaH / 1.) DMF, 0 deg C, 5 min, 2.) DMF, 23 deg C, 40 min

4: 99 percent / piperidine, acetic acid / benzene / 18 h / 23 °C

5: 94 percent / Et₃N, HCOOH, Pd(PPh₃)4 / 4 h / 23 °C

6: (PhO)2P(O)N₃, Et₃N, 4 Angstroem molecular sieves / toluene / 2 h / 70 °C

7: 1 h / 23 °C

8: 97 percent / H₂, Rh<(COD)-(R,R)-DIPAMP>(+)*BF₄(-) / 16 h / 23 °C / 2280 Torr

9: BF₃*Et₂O, H₂O / CH₂Cl₂ / 0.17 h / 0 °C

10: BF₃*Et₂O, 4 Angstroem molecular sieves / CH₂Cl₂ / 18 h / 23 °C

11: 100 percent / H₂ / 10percent Pd/C / ethyl acetate / 6 h / 23 °C / 760 Torr

12: 61 percent / HOAc / 18 h / 23 °C

13: 87 percent / Cs₂CO₃ / dimethylformamide / 1 h / 23 °C

With piperidine; tetrakis(triphenylphosphine) palladium⁽⁰⁾; n-butyllithium; formic acid; methanesulfonic acid; Rh<(COD)-(R,R)-DIPAMP>(+)*BF4(-); 4 A molecular sieve; diphenyl phosphoryl azide; boron trifluoride diethyl etherate; water; hydrogen; sodium hydride; caesium carbonate; acetic acid; triethylamine; palladium on activated charcoal; In dichloromethane; ethyl acetate; N,N-dimethyl-formamide; toluene; benzene;
DOI:10.1021/ja962480t