(C₆H₅)3GeSi(CH₃)2H

Base Information

Chemical Name:(C₆H₅)3GeSi(CH₃)2H
CAS No.:105053-60-9
Molecular Formula:C₂₀H₂₂GeSi
Molecular Weight:363.07
Hs Code.:

(C<sub>6</sub>H<sub>5</sub>)3GeSi(CH<sub>3</sub>)2H

Synonyms:(C₆H₅)3GeSi(CH₃)2H

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (C₆H₅)3GeSi(CH₃)2H

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Technology Process of (C₆H₅)3GeSi(CH₃)2H

There total 1 articles about (C₆H₅)3GeSi(CH₃)2H which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 60.0%

: 1066-35-9
dimethylmonochlorosilane

: 3005-32-1
triphenylgermanium bromide

: 105053-60-9
(C₆H₅)3GeSi(CH₃)2H

Guidance literature:: With sodium; naphtalene; In tetrahydrofuran; addn. of germane in THF and naphthalene to THF/sodium dispersion, stirred (20 h), dark green, filtered (into a pressure equilibrated dropping funnel), added dropwise to a cooled (0°C) soln. of silane in THF, green color disappeared, stirred (1 h); evapn., extn. of gummy residue (hexane/CH2Cl2 (70/30), twice), evapn., recrystn. (hexane/CH2Cl2 (90/10)); elem. anal.;
DOI:10.1016/0022-328X(86)80005-5

Reference yield: 95.0%

: 105053-60-9
(C₆H₅)3GeSi(CH₃)2H

: 105053-61-0
(C₆H₅)3GeSi(CH₃)2Cl

Guidance literature:: With chlorine; In tetrachloromethane; chlorine bubbled into a CCl4 soln. of germane until Si-H stretching frequency disappeared (monitored by IR); immediate removal of solvent, recrystn. (hexane); elem. anal.;
DOI:10.1016/0022-328X(86)80005-5