phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside]

Base Information

• Chemical Name: phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside]
• CAS No.: 220041-69-0
• Molecular Formula: C₃₂H₄₀O₁₈
• Molecular Weight: 712.659

Synonyms:phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside]

Chemical Property of phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside]

Chemical Property:

Purity/Quality:

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Technology Process of phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside]

There total 3 articles about phenyl-[O²,O³,O⁴-triacetyl-O⁶-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside] which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 73.0%

acetic anhydride (108-24-7) + phenyl-(O6-β-D-glucopyranosyl-β-D-glucopyranoside) (111468-29-2) → phenyl-[O2,O3,O4-triacetyl-O6-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside] (220041-69-0)

Guidance literature:

With pyridine; at 5 ℃;

DOI:10.1002/(SICI)1521-3765(19981204)4:12<2442::AID-CHEM2442>3.0.CO;2-A

Reference yield:

1-O-phenyl-2,3,4-tri-O-acetyl-β-D-glucopyranose (22348-21-6) + 2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide (572-09-8) → phenyl-[O2,O3,O4-triacetyl-O6-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside] (220041-69-0)

Guidance literature:

With chloroform; silver carbonate; calcium chloride;

Reference yield:

β-D-gentiobiose octaacetate (4613-78-9) + phenol (108-95-2,27073-41-2) → phenyl-[O2,O3,O4-triacetyl-O6-(tetra-O-acetyl-β-D-glucopyranosyl)-β-D-glucopyranoside] (220041-69-0)

Guidance literature:

With toluene-4-sulfonic acid;

upstream raw materials:

1-O-phenyl-2,3,4-tri-O-acetyl-β-D-glucopyranose

2,3,4,6-tetra-O-acetyl-α-D-glucopyranosyl bromide

β-D-gentiobiose octaacetate

phenol

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