1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

Base Information

Chemical Name:1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone
CAS No.:1070668-14-2
Molecular Formula:C₂₁H₂₄ClNO₃
Molecular Weight:373.879
Hs Code.:

Synonyms:1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

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Chemical Property of 1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

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Technology Process of 1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

There total 1 articles about 1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 63.0%

: 1070668-11-9
tert-butyl (3-chloro-2-methylbenzyl)carbamate

: 95092-10-7
N-methoxy-N-methyl-2-phenylacetamide

: 1070668-14-2
1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

Guidance literature:: tert-butyl (3-chloro-2-methylbenzyl)carbamate; With N,N,N,N,-tetramethylethylenediamine; sec.-butyllithium; In tetrahydrofuran; at -78 - -30 ℃; Inert atmosphere;

N-methoxy-N-methyl-2-phenylacetamide; In tetrahydrofuran; at -78 - 20 ℃;

Reference yield:

: 1070668-14-2
1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone

: 1070668-17-5
3-benzyl-5-chloro-1,2,3,4-tetrahydroisoquinoline

Guidance literature:: 1-[2-(tert-butoxycarbonylaminomethyl)-6-chlorophenyl]-3-phenyl-2-propanone; With trifluoroacetic acid; In dichloromethane; at 20 ℃; for 1h; Cooling with ice;

With sodium tetrahydroborate; In ethanol; at 20 ℃; Cooling with ice;

With water; sodium hydrogencarbonate; In ethanol;