3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

Base Information

Chemical Name:3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid
CAS No.:1154527-24-8
Molecular Formula:C₂₄H₂₈N₂O₆
Molecular Weight:440.496
Hs Code.:

Synonyms:3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

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Chemical Property of 3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

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Technology Process of 3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

There total 1 articles about 3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

: 1154527-23-7
3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid ethyl ester

: 1154527-24-8
3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

Guidance literature:: 3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid ethyl ester; With lithium hydroxide; water; In tetrahydrofuran; at 20 ℃; for 6h; Inert atmosphere;

With potassium hydrogensulfate; water; pH=2;
DOI:10.1016/j.tet.2008.08.102

Reference yield: 89.0%

: 1154527-05-5
C₁₉H₃₇NO₃Si

: 1154527-24-8
3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionic acid

: 1154527-25-9
1-[3-(6-benzyloxy-7-methoxy-1H-indol-3-yl)-2-tert-butoxycarbonylamino-propionyl]-2-[4-(tert-butyl-dimethylsilanyloxy)-3-methyl-but-2-enyl]-3-methyl-pyrrolidine-2-carboxylic acid ethyl ester

Guidance literature:: With benzotriazol-1-yloxyl-tris-(pyrrolidino)-phosphonium hexafluorophosphate; N-ethyl-N,N-diisopropylamine; In dichloromethane; at 20 ℃; for 96h;
DOI:10.1016/j.tet.2008.08.102