5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide

Base Information

Chemical Name:5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide
CAS No.:6672-63-5
Molecular Formula:C₁₄H₁₂O₂S
Molecular Weight:244.314
Hs Code.:
NSC Number:131109
DSSTox Substance ID:DTXSID30299506
Nikkaji Number:J1.402.914A,J3.076.099I
Wikidata:Q82041957

Synonyms:5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide;6672-63-5;NSC131109;DTXSID30299506;KBLXMVZQBOKWNU-UHFFFAOYSA-N;AKOS024329235;NSC-131109;Dibenz(c,E)-5,7-dihydrothiepin 6,6-dioxide;5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide #

Suppliers and Price of 5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide

Supply Marketing:

Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

Manufacturers and distributors:

Manufacture/Brand
Chemicals and raw materials
Packaging
price

Total 1 raw suppliers

Chemical Property of 5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide

Chemical Property:

Vapor Pressure:4.23E-10mmHg at 25°C
XLogP3:2.3
Hydrogen Bond Donor Count:0
Hydrogen Bond Acceptor Count:2
Rotatable Bond Count:0
Exact Mass:244.05580079
Heavy Atom Count:17
Complexity:338

Purity/Quality:: 85.0-99.8% ^*data from raw suppliers

Safty Information:

Pictogram(s):
Hazard Codes:

MSDS Files:: SDS file from LookChem

Useful:

Canonical SMILES:C1C2=CC=CC=C2C3=CC=CC=C3CS1(=O)=O

Technology Process of 5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide

There total 1 articles about 5,7-Dihydrodibenzo[c,E]thiepine 6,6-dioxide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 28.0%

: C₁₄H₈O₂S

: 6672-63-5
dibenz-1,1-dioxothiapane

: 1374583-47-7
phenyl dibenz-1,1-dioxothiapane

Guidance literature:: With cyclohexa-1,4-diene; triethylamine; In chloroform-d1; benzene; for 24h;
DOI:10.1002/asia.201100903

Reference yield:

: 6672-63-5
dibenz-1,1-dioxothiapane

: 85-01-8
phenanthrene

Guidance literature:: Multi-step reaction with 2 steps

1: 1) n-butyllithium / 1) benzene, ether, hexane, tetrahydrofuran,

2: 1) SOCl₂ / 1) benzene, 3 h, reflux, 2) 2 h

With n-butyllithium; thionyl chloride;

Reference yield:

: 6672-63-5
dibenz-1,1-dioxothiapane

: 124-38-9,18923-20-1
carbon dioxide

: 110129-22-1
6,6-dioxido-5,7-dihydrodibenzothiepin-5-carboxylic acid

: 110129-23-2
6,6-dioxido-5,7-dihydrodibenzothiepin-5,7-dicarboxylic acid

Guidance literature:: With n-butyllithium; Yield given. Multistep reaction. Yields of byproduct given; 1) benzene, ether, hexane, tetrahydrofuran,;