methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

Base Information

Chemical Name:methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate
CAS No.:1357380-76-7
Molecular Formula:C₁₄H₁₆N₄O₄
Molecular Weight:304.305
Hs Code.:

Synonyms:methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

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Chemical Property of methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

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Technology Process of methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

There total 4 articles about methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 75.0%

: 1357380-89-2
C₁₁H₁₂N₄O₂

: 1357380-76-7
methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

Guidance literature:: With potassium hydroxide; In water; dimethyl sulfoxide; at 20 ℃;
DOI:10.1002/hlca.201100189

Reference yield:

: 40814-66-2
(Z)-2-chloro-1-phenylethan-1-one oxime

: 1357380-76-7
methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

Guidance literature:: Multi-step reaction with 3 steps

1: sodium azide / water; acetone / 12 h / 20 °C

2: copper(l) iodide / tetrahydrofuran; water / Reflux

3: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; sodium azide; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; acetone; 2: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189

Reference yield:

: (Z)-2-azido-1-phenylethan-1-one oxime

: 1357380-76-7
methyl 2-{{{(1E)-2-[4-(hydroxymethyl)-1H-1,2,3-triazol-1-yl]-1-phenylethylidene}amino}oxy}acetate

Guidance literature:: Multi-step reaction with 2 steps

1: copper(l) iodide / tetrahydrofuran; water / Reflux

2: potassium hydroxide / water; dimethyl sulfoxide / 20 °C

With copper(l) iodide; potassium hydroxide; In tetrahydrofuran; water; dimethyl sulfoxide; 1: Huisgen cycloaddition;
DOI:10.1002/hlca.201100189