5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

Base Information

Chemical Name:5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate
CAS No.:72055-61-9
Molecular Formula:C₇H₈O₃S*C₁₁H₁₇N₅O₅
Molecular Weight:471.491
Hs Code.:

Synonyms:5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

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Technology Process of 5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

There total 4 articles about 5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 50507-48-7
N-Benzyloxy-1-((2R,3R,4S,5R)-3,4-dihydroxy-5-hydroxymethyl-tetrahydro-furan-2-yl)-5-formylamino-1H-imidazole-4-carboxamidine

: 72055-61-9
5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

Guidance literature:: Multi-step reaction with 2 steps

1: 86 percent / K₂CO₃ / dimethylformamide / 9 h / Ambient temperature

2: 930 mg / H₂ / Raney Ni W-2 / H₂O / 1.17 h / Ambient temperature

With hydrogen; potassium carbonate; Raney Ni W-2; In water; N,N-dimethyl-formamide;
DOI:10.1248/cpb.37.2601

Reference yield:

: 104-15-4
toluene-4-sulfonic acid

: 72055-59-5
N'-benzyloxy-5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine

: 72055-61-9
5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

Guidance literature:: With hydrogen; Raney Ni W-2; In water; for 1.16667h; Ambient temperature;
DOI:10.1248/cpb.37.2601

Reference yield:

: 72055-63-1
3-methyladenosine p-toluenesulfonate

: 72055-61-9
5-(N-methylformamido)-1-β-D-ribofuranosyl-1H-imidazole-4-carboxamidine p-tuluenesulfonate

Guidance literature:: With water; at 25 ℃; Rate constant; Equilibrium constant; at pH = 8.98; investigated by UV spectrophotometry;
DOI:10.1248/cpb.37.3243