O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

Base Information

Chemical Name:O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate
CAS No.:219122-18-6
Molecular Formula:C₃₁H₃₉O₇PS₂
Molecular Weight:618.752
Hs Code.:

Synonyms:O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

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Technology Process of O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

There total 3 articles about O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 43.0%

: 298-06-6
O,O-Diethyl hydrogen phosphorodithioate

: 1011723-04-8
glucal epoxide

: 219122-18-6
O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

: 219122-17-5
O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-α-D-glucopyranoside phosphorodithioate

Guidance literature:: In dichloromethane; at -78 - 20 ℃; for 1.5h;
DOI:10.1021/ja016227r

Reference yield:

: 55628-54-1
3,4,6-tri-O-benzyl-D-glucal

: 219122-18-6
O,O-diethyl 3,4,6-tri-O-benzyl-1-thio-β-D-glucopyranoside phosphorodithioate

Guidance literature:: Multi-step reaction with 2 steps

1: dimethyldioxirane / CH₂Cl₂; acetone / 0.25 h / 0 °C

2: 39 percent / CH₂Cl₂ / 1.5 h / -78 - 20 °C

With 3,3-dimethyldioxirane; In dichloromethane; acetone;
DOI:10.1021/ja016227r