5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

Base Information

Chemical Name:5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide
CAS No.:1198621-30-5
Molecular Formula:C₂₉H₂₇F₂N₃O₄
Molecular Weight:519.548
Hs Code.:

Synonyms:5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

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Chemical Property of 5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

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Technology Process of 5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

There total 5 articles about 5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 17.0%

: 1198621-66-7
N,7-bis(benzyloxy)-3-hydroxy-1,3-dihydrofuro[3,4-c]pyridine-6-carboxamide

: 90390-27-5
3,5-difluorobenzylamine

: 1198621-30-5
5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

Guidance literature:: With sodium cyanoborohydride; In ethanol; at 20 ℃;

Reference yield:

: 1198621-04-3
N,3-bis(benzyloxy)-4,5-bis(hydroxymethyl)picolinamide

: 1198621-30-5
5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

Guidance literature:: Multi-step reaction with 2 steps

1: manganese(IV) oxide / dichloromethane / 20 °C

2: sodium cyanoborohydride / ethanol / 20 °C

With manganese(IV) oxide; sodium cyanoborohydride; In ethanol; dichloromethane;

Reference yield:

: 1198621-03-2
N,9-bis(benzyloxy)-3,3-dimethyl-1,5-dibydro-[1,3]dioxepino[5,6-c]pyridine-8-carboxamide

: 1198621-30-5
5-((3,5-difluorobenzylamino)methyl)-N,3-bis(benzyloxy)-4-(hydroxymethyl)picolinainide

Guidance literature:: Multi-step reaction with 3 steps

1: formic acid / tetrahydrofuran; water / 2 h / 70 °C

2: manganese(IV) oxide / dichloromethane / 20 °C

3: sodium cyanoborohydride / ethanol / 20 °C

With manganese(IV) oxide; formic acid; sodium cyanoborohydride; In tetrahydrofuran; ethanol; dichloromethane; water;