1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Base Information

Chemical Name:1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol
CAS No.:114126-54-4
Molecular Formula:C₂₇H₃₆N₂O₆S₂
Molecular Weight:548.725
Hs Code.:

1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis<N-(p-tolylsulfonyl)amino>-3,4-O-(1-methylethylidene)-L-iditol

Synonyms:1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of 1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

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Technology Process of 1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

There total 2 articles about 1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 80.0%

: 109075-06-1
(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine

: 114126-54-4
1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Guidance literature:: In tetrahydrofuran; at -78 - 0 ℃; for 1h;
DOI:10.1016/S0040-4039(00)95507-2

Reference yield:

: 917-57-7
vinyllithium

: 109075-06-1
(S)-2-((4R,5R)-2,2-dimethyl-5-((S)-1-tosylaziridin-2-yl)-1,3-dioxolan-4-yl)-1-tosyl-aziridine

: 114126-54-4
1,2,5,6-tetradeoxy-1,6-divinyl-2,5-bis-3,4-O-(1-methylethylidene)-L-iditol

Guidance literature:: With 1.) CuCN; Yield given. Multistep reaction; 1.) THF, Et₂O, pentane, from -78 to 0 deg C, 2.) THF, Et₂O, pentane, from -78 to 0 deg C, 1 h;
DOI:10.1021/jo00283a028