(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

Base Information

Chemical Name:(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid
CAS No.:92270-40-1
Molecular Formula:C₁₈H₁₃Cl₃INO₆
Molecular Weight:572.568
Hs Code.:

Synonyms:(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

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Chemical Property of (2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

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Technology Process of (2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

There total 3 articles about (2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 78235-49-1
2,3-dichloro-4-<3-<(2-chloroacetamido)methyl>-4-hydroxybenzoyl>phenoxyacetic acid

: 92270-40-1
(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

Guidance literature:: With Iodine monochloride; In acetic acid; at 75 ℃; for 20h;
DOI:10.1021/jm00378a010

Reference yield:

: 62967-00-4
2,3-dichloro-4-(4'-hydroxybenzoyl)-phenoxyacetic acid

: 92270-40-1
(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 2 steps

1: CH₃SO₃H / 3 h / Ambient temperature

2: ICl / acetic acid / 20 h / 75 °C

With methanesulfonic acid; Iodine monochloride; In acetic acid;
DOI:10.1021/jm00378a010

Reference yield:

: 75554-04-0
ethyl 2,3-dichloro-4-(4-nitrobenzoyl)phenoxyacetate

: 92270-40-1
(2,3-Dichloro-4-{3-[(2-chloro-acetylamino)-methyl]-4-hydroxy-5-iodo-benzoyl}-phenoxy)-acetic acid

Guidance literature:: Multi-step reaction with 3 steps

1: acetaldoxime, NaOH / dimethylformamide / 18 h / Ambient temperature

2: CH₃SO₃H / 3 h / Ambient temperature

3: ICl / acetic acid / 20 h / 75 °C

With sodium hydroxide; Acetaldehyde oxime; methanesulfonic acid; Iodine monochloride; In acetic acid; N,N-dimethyl-formamide;
DOI:10.1021/jm00378a010