(S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol

Base Information

• Chemical Name: (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol
• CAS No.: 221493-41-0
• Molecular Formula: C₂₀H₃₃N₃O₄S
• Molecular Weight: 411.566

Synonyms:(S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol

Chemical Property of (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol

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Technology Process of (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol

There total 3 articles about (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 99.0%

N-[1-[(S)-1-(2-Hydroxy-ethyl)-5-methyl-hex-4-enylamino]-1-methylsulfanyl-meth-(Z)-ylidene]-4-methoxy-2,3,6-trimethyl-benzenesulfonamide (221493-39-6) → (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol (221493-41-0)

Guidance literature:

With ammonia; silver nitrate; In acetonitrile; at 0 - 20 ℃; for 18h;

DOI:10.1021/jo981972g

Reference yield:

(S)-3-amino-7-methyl-6-octen-1-ol (162145-93-9) → (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol (221493-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / benzene / 2 h / Heating

2: 99 percent / NH₃, AgNO₃ / acetonitrile / 18 h / 0 - 20 °C

With ammonia; silver nitrate; In acetonitrile; benzene;

DOI:10.1021/jo981972g

Reference yield:

S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate (221493-37-4) → (S)-N-<(aminomethylene)-4-methoxy-2,3,6-trimethylbenzenesulfonamide>-3-amino-7-methyl-6-octenol (221493-41-0)

Guidance literature:

Multi-step reaction with 2 steps

1: 77 percent / benzene / 2 h / Heating

2: 99 percent / NH₃, AgNO₃ / acetonitrile / 18 h / 0 - 20 °C

With ammonia; silver nitrate; In acetonitrile; benzene;

DOI:10.1021/jo981972g

upstream raw materials:

N-[1-[(S)-1-(2-Hydroxy-ethyl)-5-methyl-hex-4-enylamino]-1-methylsulfanyl-meth-(Z)-ylidene]-4-methoxy-2,3,6-trimethyl-benzenesulfonamide

(S)-3-amino-7-methyl-6-octen-1-ol

S,S-dimethyl N-(4-methoxy-2,3,6-trimethylbenzenesulfonyl)-carbonimidodithioate

Downstream raw materials:

N-[1-Amino-1-[(S)-2-hydroxy-5-(2-hydroxy-ethyl)-pyrrolidin-1-yl]-meth-(E)-ylidene]-4-methoxy-2,3,6-trimethyl-benzenesulfonamide

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