2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

Base Information

Chemical Name:2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine
CAS No.:161001-94-1
Molecular Formula:C₂₆H₂₈N₆O₁₁
Molecular Weight:600.542
Hs Code.:

2',3',5'-tri-O-acetyl-N<sup>6</sup>-methyl-N<sup>6</sup>-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

Synonyms:2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

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Chemical Property of 2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

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Technology Process of 2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

There total 7 articles about 2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 93.0%

: 56787-20-3
2',3',5'-tri-O-acetyl-N⁶-methyl-adenosine

: 161001-95-2
2-(4-nitrophenyl)ethyl 2H-tetrazole-2-carboxylate

: 161001-94-1
2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

Guidance literature:: In 1,4-dioxane; at 50 ℃; for 18h;
DOI:10.1002/hlca.19940770509

Reference yield: 35.0%

: 88091-68-3
2-(4-nitrophenyl)ethoxycarbonyl chloride

: 56787-20-3
2',3',5'-tri-O-acetyl-N⁶-methyl-adenosine

: 161001-94-1
2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

Guidance literature:: With pyridine; dmap; In dichloromethane; at 60 ℃; for 24h;
DOI:10.1002/hlca.19940770509

Reference yield:

: 1867-73-8
N⁶-methyladenosine

: 161001-94-1
2',3',5'-tri-O-acetyl-N⁶-methyl-N⁶-<2-(4-nitrophenyl)ethoxycarbonyl>adenosine

Guidance literature:: Multi-step reaction with 2 steps

1: 90 percent / pyridine / 2 h

2: 35 percent / pyridine, DMAP / CH₂Cl₂ / 24 h / 60 °C

With pyridine; dmap; In dichloromethane;
DOI:10.1002/hlca.19940770509