C₅₂H₇₃Cl₃O₈SSi

Base Information

Chemical Name:C₅₂H₇₃Cl₃O₈SSi
CAS No.:736170-32-4
Molecular Formula:C₅₂H₇₃Cl₃O₈SSi
Molecular Weight:992.657
Hs Code.:

C<sub>52</sub>H<sub>73</sub>Cl<sub>3</sub>O<sub>8</sub>SSi

Synonyms:C₅₂H₇₃Cl₃O₈SSi

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of C₅₂H₇₃Cl₃O₈SSi

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Technology Process of C₅₂H₇₃Cl₃O₈SSi

There total 3 articles about C₅₂H₇₃Cl₃O₈SSi which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 85.0%

: 75-08-1
ethanethiol

: 736170-31-3
(2S,5aS,7R,8S,10aR)-2-[(2R,3S,4S,6R)-4-Benzyloxy-6-(3-benzyloxy-propyl)-3-hydroxy-tetrahydro-pyran-2-ylmethyl]-8-(tert-butyl-dimethyl-silanyloxy)-8-methyl-7-[3-(2,4,6-trichloro-benzyloxy)-propyl]-octahydro-1,6-dioxa-heptalen-3-one

: 736170-32-4
C₅₂H₇₃Cl₃O₈SSi

Guidance literature:: With zinc trifluoromethanesulfonate; In dichloromethane; at 0 - 23 ℃; for 6.5h;
DOI:10.1016/j.tetlet.2004.05.020

Reference yield:

: 736170-30-2
2-[4-benzyloxy-6-(3-benzyloxy-propyl)-3-(naphthalen-2-ylmethoxy)-tetrahydro-pyran-2-ylmethyl]-8-(tert-butyl-dimethyl-silanyloxy)-8-methyl-7-[3-(2,4,6-trichloro-benzyloxy)-propyl]-octahydro-1,6-dioxa-heptalen-3-one

: 736170-32-4
C₅₂H₇₃Cl₃O₈SSi

Guidance literature:: Multi-step reaction with 2 steps

1: 93 percent / DDQ / CH₂Cl₂; methanol; H₂O / 1 h / 0 - 25 °C

2: 85 percent / Zn(OTf)2 / CH₂Cl₂ / 6.5 h / 0 - 23 °C

With zinc trifluoromethanesulfonate; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2004.05.020

Reference yield:

: 736170-29-9
2-[4-benzyloxy-6-(3-benzyloxy-propyl)-3-(naphthalen-2-ylmethoxy)-tetrahydro-pyran-2-ylmethyl]-8-(tert-butyl-dimethyl-silanyloxy)-8-methyl-7-[3-(2,4,6-trichloro-benzyloxy)-propyl]-decahydro-1,6-dioxa-heptalen-3-ol

: 736170-32-4
C₅₂H₇₃Cl₃O₈SSi

Guidance literature:: Multi-step reaction with 3 steps

1: 100 percent / Dess-Martin periodinane / CH₂Cl₂ / 1 h / 25 °C

2: 93 percent / DDQ / CH₂Cl₂; methanol; H₂O / 1 h / 0 - 25 °C

3: 85 percent / Zn(OTf)2 / CH₂Cl₂ / 6.5 h / 0 - 23 °C

With zinc trifluoromethanesulfonate; Dess-Martin periodane; 2,3-dicyano-5,6-dichloro-p-benzoquinone; In methanol; dichloromethane; water;
DOI:10.1016/j.tetlet.2004.05.020