(+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene

Base Information

• Chemical Name: (+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene
• CAS No.: 90858-23-4
• Molecular Formula: C₂₁H₃₂O₂
• Molecular Weight: 316.484

Synonyms:(+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene

Chemical Property of (+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene

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Technology Process of (+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene

There total 1 articles about (+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 46.0%

2,6,6-trimethylcyclohex-1-enecarbaldehyde (432-25-7) + 2-Methoxy-5-isopropylbenzyl chloride (22252-69-3) → (+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene (90858-23-4)

Guidance literature:

With sodium naphthalenide; In tetrahydrofuran; at -5 ℃; for 2h;

DOI:10.1021/jo00190a038

Reference yield: 84.0%

(+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene (90858-23-4) → 4-Isopropyl-1-methoxy-2-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-benzene (90858-24-5)

Guidance literature:

With lithium aluminium tetrahydride; aluminium trichloride; In diethyl ether; for 1h; Ambient temperature;

DOI:10.1021/jo00190a038

Reference yield: 69.0%

(+/-)-1-<2-(2-Methoxy-5-isopropylphenyl)-1-hydroxyethyl>-2,6,6-trimethylcyclohexene (90858-23-4) → 2-(2,6,6-Trimethyl-1-cyclohexenyl)-1-(2-methoxy-5-isopropylphenyl)ethane (90858-25-6)

Guidance literature:

With triethylsilane; boron trifluoride diethyl etherate; In dichloromethane; at -10 ℃; for 1h;

DOI:10.1021/jo00190a038

upstream raw materials:

2,6,6-trimethylcyclohex-1-enecarbaldehyde

2-Methoxy-5-isopropylbenzyl chloride

Downstream raw materials:

4-Isopropyl-1-methoxy-2-[(E)-2-(2,6,6-trimethyl-cyclohex-1-enyl)-vinyl]-benzene

2-(2,6,6-Trimethyl-1-cyclohexenyl)-1-(2-methoxy-5-isopropylphenyl)ethane

2-(2,6,6-Trimethyl-1-cyclohexenyl)-1-(2-hydroxy-5-isopropylphenyl)ethane

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