(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

Base Information

Chemical Name:(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid
CAS No.:1440433-93-1
Molecular Formula:C₁₇H₂₂N₂O₆
Molecular Weight:350.371
Hs Code.:

Synonyms:(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

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Business phase:: The product has achieved commercial mass production^*data from LookChem market partment

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Chemical Property of (S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

Chemical Property:

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Technology Process of (S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

There total 6 articles about (S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 1440434-03-6
C₂₂H₂₈N₂O₈

: 1440433-93-1
(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

Guidance literature:: With methanol; sodium hydroxide; In water; at 20 ℃; for 0.25h;
DOI:10.1016/j.bmcl.2013.04.033

Reference yield:

: 5874-75-9
methyl (2S)-2-amino-5-[[(benzyloxy)carbonyl]amino]pentanoate hydrochloride

: 1440433-93-1
(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

Guidance literature:: Multi-step reaction with 4 steps

1: sodium hydrogencarbonate / tetrahydrofuran; water / 2 h / 20 °C

2: acetic acid; hydrogen; palladium 10% on activated carbon / methanol / 20 °C

3: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C

4: methanol; sodium hydroxide / water / 0.25 h / 20 °C

With methanol; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmcl.2013.04.033

Reference yield:

: 1440433-99-7
C₁₇H₂₄N₂O₅

: 1440433-93-1
(S,E)-5-(3-(3,4-dihydroxyphenyl)acrylamido)-2-propionamidopentanoic acid

Guidance literature:: Multi-step reaction with 3 steps

1: acetic acid; hydrogen; palladium 10% on activated carbon / methanol / 20 °C

2: sodium hydrogencarbonate / tetrahydrofuran; water / 20 °C

3: methanol; sodium hydroxide / water / 0.25 h / 20 °C

With methanol; palladium 10% on activated carbon; hydrogen; sodium hydrogencarbonate; acetic acid; sodium hydroxide; In tetrahydrofuran; methanol; water;
DOI:10.1016/j.bmcl.2013.04.033