N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide

Base Information

• Chemical Name: N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide
• CAS No.: 1228507-43-4
• Molecular Formula: C₁₈H₁₃F₆N₃S
• Molecular Weight: 417.378

Synonyms:N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide

Chemical Property of N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide

Chemical Property:

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Technology Process of N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide

There total 1 articles about N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 97.0%

N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzamide (1228507-42-3) → N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide (1228507-43-4)

Guidance literature:

With Lawessons reagent; In toluene; for 16h; Inert atmosphere; Reflux;

DOI:10.1002/chem.200902912

Reference yield:

N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide (1228507-43-4) + tetrabutylammonium dihydrogen phosphate (5574-97-0) → C18H12F6N3S(1-)*C16H36N(1+)

Guidance literature:

In acetonitrile; Equilibrium constant;

DOI:10.1039/c7ob01704a

Reference yield:

N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzothioamide (1228507-43-4) + tetrabutylammonium benzoate (18819-89-1) → C18H12F6N3S(1-)*C16H36N(1+)

Guidance literature:

In acetonitrile; Equilibrium constant;

DOI:10.1039/c7ob01704a

upstream raw materials:

N-(5,6-dimethyl-1H-benzimidazol-2-yl)-3,5-bis(trifluoromethyl)benzamide

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