dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II)

Base Information

• Chemical Name: dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II)
• CAS No.: 1428980-38-4
• Molecular Formula: C₂₇H₄₃Cl₂PRuSi
• Molecular Weight: 598.674

Synonyms:dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II)

Chemical Property of dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II)

Chemical Property:

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Technology Process of dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II)

There total 2 articles about dichloro(η⁶-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II) which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

[ruthenium(II)(η6-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]2 (52462-29-0) + cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine → dichloro(η6-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II) (1428980-38-4)

Guidance literature:

at 20 ℃; for 0.5h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om3012294

Reference yield:

chloroform-d1 (865-49-6) + C27H45PRuSi (1428980-53-3) → dichloro(η6-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II) (1428980-38-4)

Guidance literature:

Inert atmosphere; Schlenk technique;

DOI:10.1021/om3012294

Reference yield: 90.0%

dichloro(η6-p-cymene)[cyclohexyl(2,2-dimethyl-3-phenyl-2-sila-1-propyl)methylphosphine]ruthenium(II) (1428980-38-4) → dichloro[κ-P-η6-cyclohexyl((benzyldimethylsilyl)methyl)methylphosphine]ruthenium(II) (1428980-50-0)

Guidance literature:

In chlorobenzene; at 130 ℃; for 4h; Inert atmosphere; Schlenk technique;

DOI:10.1021/om3012294

upstream raw materials:

chloroform-d1

C₂₇H₄₅PRuSi

[ruthenium(II)(η⁶-1-methyl-4-isopropyl-benzene)(chloride)(μ-chloride)]₂

Downstream raw materials:

C₂₇H₄₅PRuSi

dichloro[κ-P-η⁶-cyclohexyl((benzyldimethylsilyl)methyl)methylphosphine]ruthenium(II)

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