<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

Base Information

Chemical Name:<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate
CAS No.:124483-22-3
Molecular Formula:C₂₈H₂₉NO₆
Molecular Weight:475.541
Hs Code.:

Synonyms:<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

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Chemical Property of <(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

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Technology Process of <(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

There total 6 articles about <(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 29.0%

: 20698-91-3
(R)-methyl mandelate

: 106868-58-0
2(R,S)-(4-morpholinylcarbonylmethyl)-3-(1-naphthyl)-propionic Acid

: 124483-21-2
<(1S)-1-Methoxycarbonyl)benzyl> (-)-3-(Morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

: 124483-22-3
<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In chloroform; 1.)0 deg C, 2 h, 2.)25 deg C,;
DOI:10.1021/jo00292a052

Reference yield: 28.0%

: 21210-43-5
(S)-Methyl mandelate

: 106868-58-0
2(R,S)-(4-morpholinylcarbonylmethyl)-3-(1-naphthyl)-propionic Acid

: 124483-21-2
<(1S)-1-Methoxycarbonyl)benzyl> (-)-3-(Morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

: 124483-22-3
<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

Guidance literature:: With dicyclohexyl-carbodiimide; dmap; In chloroform; 1.)0 deg C, 2 h, 2.)25 deg C,;
DOI:10.1021/jo00292a052

Reference yield:

: 103632-75-3
2-(1-Naphthylmethylidene)succinic anhydride

: 124483-22-3
<(1R)-1-(Methoxycarbonyl)benzyl> (+)-3-(morpholinocarbonyl)-2-(1-naphthylmethyl)propionate

Guidance literature:: Multi-step reaction with 3 steps

1: 84 percent / ethyl acetate

2: 97.5 percent / H₂ / 10percent Pd/C / methanol / 760 Torr

3: 1,3-dicyclohexylcarbodiimide / (N,N-dimethylamino)pyridine / CHCl₃ / 1.)0 deg C, 2 h, 2.)25 deg C,

With hydrogen; dicyclohexyl-carbodiimide; dmap; palladium on activated charcoal; In methanol; chloroform; ethyl acetate;
DOI:10.1021/jo00292a052