TERT-AMYL METHYL SULPHIDE

Base Information

• Chemical Name: TERT-AMYL METHYL SULPHIDE
• CAS No.: 13286-92-5
• Molecular Formula: C₆H₁₄S
• Molecular Weight: 118.243
• Hs Code.: 2930909090
• Mol file: 13286-92-5.mol

Synonyms:Sulfide,methyl tert-pentyl (7CI,8CI);Methyl tert-pentyl sulfide;

Chemical Property of TERT-AMYL METHYL SULPHIDE

Chemical Property:

• Melting Point: -96.69°C (estimate)
• Refractive Index: 1.4301 (estimate)
• Boiling Point: 121.4 °C at 760 mmHg
• Flash Point: 8.5 °C
• PSA: 25.30000
• Density: 0.835 g/cm³
• LogP: 2.39550

Purity/Quality:

98%Min ^*data from raw suppliers

Safty Information:

• Pictogram(s): R10:Flammable.
• Hazard Codes: R10:Flammable.
• Statements: R10:Flammable.
• Safety Statements: S23:Do not inhale gas/fumes/vapour/spray.; S24/25:Avoid contact with skin and eyes.

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of TERT-AMYL METHYL SULPHIDE

There total 2 articles about TERT-AMYL METHYL SULPHIDE which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

1,1-dimethylpropanethiol (1679-09-0) + methyl iodide (74-88-4) → 2-methyl-2-(methylthio)butane (13286-92-5)

Guidance literature:

1,1-dimethylpropanethiol; With n-butyllithium; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.166667h; Inert atmosphere;

methyl iodide; In tetrahydrofuran; hexane; at 0 - 20 ℃; for 0.333333h; Inert atmosphere;

DOI:10.1021/jf506135c

Reference yield:

→ 2-methyl-2-(methylthio)butane (13286-92-5)

Guidance literature:

tert-Amylmercaptan, CH3Br;

upstream raw materials:

1,1-dimethylpropanethiol

methyl iodide

Refernces

• 1、 Kawata,Harano,Taguchi. "Catalytic rearrangement of O,S-dialkyl dithiocarbonates to S,S-dialkyl dithiocarbonates. II. The effects of structure of O,S-dialkyl dithiocarbonates, catalysts and solvents (author's transl)". . p. 832 - 840,835,836,838. Retrieved 2007/10/12.