N-(4-CHLOROPHENYL)ANTHRANILIC ACID

Base Information

• Chemical Name: N-(4-CHLOROPHENYL)ANTHRANILIC ACID
• CAS No.: 13278-35-8
• Molecular Formula: C13H10 Cl N O2
• Molecular Weight: 247.681
• Hs Code.: 2922499990
• Mol file: 13278-35-8.mol

Synonyms:Anthranilicacid, N-(p-chlorophenyl)- (7CI,8CI); 2-(4-Chloroanilino)benzoic acid;N-(4-Chlorophenyl)anthranilic acid; N-(4'-Chlorophenyl)anthranilic acid;N-(p-Chlorophenyl)anthranilic acid

Chemical Property of N-(4-CHLOROPHENYL)ANTHRANILIC ACID

Chemical Property:

• Melting Point: 177-178 °C
• Boiling Point: 407.5±30.0 °C(Predicted)
• PKA: 3.66±0.36(Predicted)
• PSA: 49.33000
• Density: 1.376±0.06 g/cm3(Predicted)
• LogP: 3.85480

Purity/Quality:

99% ^*data from raw suppliers

2-(4-Chloroanilino)benzoic acid ^*data from reagent suppliers

Safty Information:

• Pictogram(s):  
• Hazard Codes: 

MSDS Files:

SDS file from LookChem

Useful:

Technology Process of N-(4-CHLOROPHENYL)ANTHRANILIC ACID

There total 14 articles about N-(4-CHLOROPHENYL)ANTHRANILIC ACID which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 96.0%

2-Iodobenzoic acid (88-67-5) + 4-chloro-aniline (106-47-8) → 2-(4-chloroanilino)benzoic acid (13278-35-8)

Guidance literature:

With potassium carbonate; CuPy₂Cl₂; at 75 ℃; for 0.333333h; microwave irradiation;

DOI:10.3184/030823407X255597

Reference yield: 94.0%

4-chloro-aniline (106-47-8) + 2-bromobenzoic-acid (88-65-3) → 2-(4-chloroanilino)benzoic acid (13278-35-8)

Guidance literature:

With potassium carbonate; CuPy₂Cl₂; at 75 ℃; for 0.333333h; microwave irradiation;

DOI:10.3184/030823407X255597

Reference yield: 84.0%

4-chloro-aniline (106-47-8) + ortho-chlorobenzoic acid (118-91-2) → 2-(4-chloroanilino)benzoic acid (13278-35-8)

Guidance literature:

With copper; potassium carbonate; In i-Amyl alcohol; for 6h; Heating;

DOI:10.1016/j.bmc.2007.09.020

upstream raw materials:

methyl 2-[N-(4-chlorophenyl)benzamido]benzoate

potassium 2-chlorobenzoate

4-chloro-aniline

ortho-chlorobenzoic acid

Downstream raw materials:

2,9-dichloroacridine

1-(4-chlorophenyl)-1,2-dihydro-(4H)-3,1-benzoxazin-4-one

2-(4-Chloro-phenylamino)-benzoic acid 2-[(E)-2,4-dioxo-imidazolidin-1-ylimino]-ethyl ester

2-((4-chlorophenyl)amino)benzamide

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