C₃₇H₅₅N₃O₈

Base Information

Chemical Name:C₃₇H₅₅N₃O₈
CAS No.:1369430-92-1
Molecular Formula:C₃₇H₅₅N₃O₈
Molecular Weight:669.859
Hs Code.:

C<sub>37</sub>H<sub>55</sub>N<sub>3</sub>O<sub>8</sub>

Synonyms:C₃₇H₅₅N₃O₈

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Chemical Property of C₃₇H₅₅N₃O₈

Chemical Property:

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Technology Process of C₃₇H₅₅N₃O₈

There total 23 articles about C₃₇H₅₅N₃O₈ which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield: 98.0%

: 1369430-91-0
C₄₇H₆₅N₃O₁₃

: 1369430-92-1
C₃₇H₅₅N₃O₈

Guidance literature:: With methanol; sodium methylate; at 20 ℃; for 1h; Product distribution / selectivity;

Reference yield:

: 618-45-1
3-isopropylhydroxybenzene

: 1369430-92-1
C₃₇H₅₅N₃O₈

Guidance literature:: Multi-step reaction with 10 steps

1.1: bromine / acetic acid / 1.53 h / 19 - 20 °C / Cooling with ice

2.1: N-ethyl-N,N-diisopropylamine / chloroform / 2 h / 20 °C / Cooling

3.1: n-butyllithium / tetrahydrofuran; hexane / 0.92 h / -86 - -74 °C / Inert atmosphere

3.2: 1.47 h / -86 - -74 °C

4.1: methanesulfonic acid / methanol / 1 h / Reflux

5.1: acetic anhydride; N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 21 h / 20 °C

6.1: trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane / water; acetonitrile / 1.5 h / Cooling

6.2: 0.42 h / Cooling

7.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 3 h / Inert atmosphere; Reflux

8.1: benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine / N,N-dimethyl-formamide / 11 h / 20 °C

9.1: trifluoroacetic acid / chloroform / 20.17 h / 20 °C

10.1: methanol; sodium methylate / 1 h / 20 °C

With methanol; n-butyllithium; methanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane; bromine; sodium methylate; acetic anhydride; benzotriazol-1-ol; 1-ethyl-(3-(3-dimethylamino)propyl)-carbodiimide hydrochloride; triethylamine; N-ethyl-N,N-diisopropylamine; trifluoroacetic acid; dmap; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; hexane; chloroform; water; acetic acid; N,N-dimethyl-formamide; acetonitrile; 7.1: Heck Reaction;

Reference yield:

: 1359948-56-3
C₄₀H₇₃BrO₉Si₅

: 1369430-92-1
C₃₇H₅₅N₃O₈

Guidance literature:: Multi-step reaction with 6 steps

1.1: methanesulfonic acid / methanol / 1 h / Reflux

2.1: acetic anhydride; N-ethyl-N,N-diisopropylamine / dmap / tetrahydrofuran / 21 h / 20 °C

3.1: trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane / water; acetonitrile / 1.5 h / Cooling

3.2: 0.42 h / Cooling

4.1: triethylamine / palladium diacetate; tris-(o-tolyl)phosphine / acetonitrile / 0.33 h / 120 °C / Microwave irradiation; Inert atmosphere

5.1: 1,1'-carbonyldiimidazole / chloroform / 1 h / 20 °C

5.2: 18 h / 20 °C

6.1: methanol; sodium methylate / 1 h / 20 °C

With methanol; methanesulfonic acid; trimethylsilyl trifluoromethanesulfonate; tert-butyldimethylsilane; sodium methylate; acetic anhydride; triethylamine; N-ethyl-N,N-diisopropylamine; 1,1'-carbonyldiimidazole; dmap; palladium diacetate; tris-(o-tolyl)phosphine; In tetrahydrofuran; methanol; chloroform; water; acetonitrile; 4.1: Heck Reaction;