N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

Base Information

Chemical Name:N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester
CAS No.:863296-94-0
Molecular Formula:C₁₂H₁₄F₂N₂O₂S
Molecular Weight:288.318
Hs Code.:

Synonyms:N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

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Chemical Property of N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

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Technology Process of N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

There total 4 articles about N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: C₁₂H₁₄F₂N₂O₃

: 863296-94-0
N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: With Lawessons reagent; In tetrahydrofuran; at 80 ℃; for 0.333333h; microwave irradiation;
DOI:10.1021/jm070453f

Reference yield:

: 870-46-2
t-butoxycarbonylhydrazine

: 863296-94-0
N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: EDC; N,N-dimethylaminopyridine / dimethylformamide; tetrahydrofuran / 3 h

2: Lawesson's reagent / tetrahydrofuran / 0.33 h / 80 °C / microwave irradiation

With Lawessons reagent; dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm070453f

Reference yield:

: 455-86-7
3,4-Difluorobenzoic acid

: 863296-94-0
N'-(3,4-Difluoro-thiobenzoyl)-hydrazinecarboxylic acid tert-butyl ester

Guidance literature:: Multi-step reaction with 2 steps

1: EDC; N,N-dimethylaminopyridine / dimethylformamide; tetrahydrofuran / 3 h

2: Lawesson's reagent / tetrahydrofuran / 0.33 h / 80 °C / microwave irradiation

With Lawessons reagent; dmap; N-(3-dimethylaminopropyl)-N-ethylcarbodiimide; In tetrahydrofuran; N,N-dimethyl-formamide;
DOI:10.1021/jm070453f