4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

Base Information

Chemical Name:4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone
CAS No.:1265594-39-5
Molecular Formula:C₁₉H₁₅F₃O₅
Molecular Weight:380.32
Hs Code.:

Synonyms:4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

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Chemical Property of 4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

Chemical Property:

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Technology Process of 4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

There total 4 articles about 4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone which guide to synthetic route it. The literature collected by LookChem mainly comes from the sharing of users and the free literature resources found by Internet computing technology. We keep the original model of the professional version of literature to make it easier and faster for users to retrieve and use. At the same time, we analyze and calculate the most feasible synthesis route with the highest yield for your reference as below:

synthetic route:

Reference yield:

: 209991-63-9
2,4,6-trifluorophenylacetic acid

: 72661-28-0
α-bromo-3,5-dimethoxypropiophenone

: 1265594-39-5
4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

Guidance literature:: 2,4,6-trifluorophenylacetic acid; α-bromo-3,5-dimethoxypropiophenone; With triethylamine; In acetonitrile;

With 1,8-diazabicyclo[5.4.0]undec-7-ene; In acetonitrile; for 1h;

In acetonitrile; for 3h;

Reference yield:

: 41497-31-8
3,5-dimethoxyphenyl ethyl ketone

: 1265594-39-5
4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

Guidance literature:: Multi-step reaction with 2 steps

1.1: copper(ll) bromide / chloroform; acetonitrile / 6 h / Reflux

2.1: triethylamine / acetonitrile

2.2: 1 h

2.3: air / 3 h

With triethylamine; copper(ll) bromide; In chloroform; acetonitrile;

Reference yield:

: 17213-57-9
3,5-dimethoxybenzoyl chloride

: 1265594-39-5
4-(3,5-dimethoxyphenyl)-5-hydroxy-5-methyl-3-(2,4,6-trifluorophenyl)-2(5H)-furanone

Guidance literature:: Multi-step reaction with 4 steps

1.1: triethylamine / dichloromethane; tetrahydrofuran / -10 - 20 °C

2.1: tetrahydrofuran / 0 - 20 °C

3.1: copper(ll) bromide / chloroform; acetonitrile / 6 h / Reflux

4.1: triethylamine / acetonitrile

4.2: 1 h

4.3: air / 3 h

With triethylamine; copper(ll) bromide; In tetrahydrofuran; dichloromethane; chloroform; acetonitrile;